Web Analytics

Pyrolysis Gas Chromatography/Mass Spectrometry

Pyrolysis Gas Chromatography/Mass Spectrometry (Pyro-GC-MS)

Pyrolysis GC-MS: Characterize non-analyzable polymers and composite materials

Pyrolysis Gas Chromatography/Mass Spectrometry (Pyro-GC-MS) is a very highly sensitive analytical tool that is used to characterize the polymers and composite materials that cannot be analyzed. For this process to occur, the traditional GC-MS technique is used.

Overview of (Pyro-GC-MS)

A sample is taken to the heated environment, and then it breaks down into smaller components & fragments. The components are thus named pyrolyzates, which are then analyzed and chromatographically separated like traditional GC-MS. The intrinsic affinity of the compound is utilized when the components are separated. After the separation of pyrolyzates, analysis of data is undertaken.

White Paper Download

Failure mode effects Investigation

Download

Risk and Failure analysis, Mitigation and Corrective services.

Types of Pyrolysis-GC-MS Analysis
  • Single Shot Pyrolysis-GC-MS: It runs on a single temperature, which is then rapidly increased at a rate of 20 msec to break bonds.
  • Double Shot Pyrolysis: It runs both at high and low temperatures. The latter part is known as the thermal desorption step. It examines low molecular weight components, residual solvents, and additives.
  • Evolved Gas Analysis: The same sample is put into the Pyrolysis unit which is set at a low temperature. The temperature is then increased, and the component is evolved. This testing helps to determine the temperature range of the desired component.
  • Low-Temperature Thermal Desorption: It takes place for products such as residual solvents, additives, and other off-gassed components. Here, in this case, polymer identification is not required.
  • Reactive Pyrolysis: Data interpretation of complex mixtures is difficult. For example, for certain classes of compounds, such as polyesters. A chemical reaction occurs when the derivatization technique is utilized. A pyrolysis chamber is a chemical reaction that allows easy interpretation of the products.
  • Quantitative Pyrolysis-GC-MS: When the amount is not calculated using another technique, then this testing approach is used. An example component such as Irganox, Irgafos have low ppm additive.
  • CyrotrappingPyrolysis-GC-MS: This testing technique is used to narrow down the chromatographic band and then improve the detection limit of the sample, which is cryptrapped with the help of liquid nitrogen.
Industries Served
  • Aerospace
  • Automotive
  • Biomedical/biotechnology
  • Compound Semiconductor
  • Data Storage
  • Defense
  • Displays
  • Electronics
  • Industrial Products
  • Lighting
  • Pharmaceutical
  • Photonics
  • Polymer
  • Semiconductor
  • Solar Photovoltaics
  • Telecommunications
Why Choose Pyrolysis-GC-MS

Several strengths are associated with the technique. These are as follows-

  • Capable of examining compounds and materials which are not appropriate for other traditional GC-MS
  • The analysis is done with micrograms of samples
  • Reduction of sample preparation
  • Ability to reach multiple block polymers due to effective study of polymeric structures

Nishka Research Centre

Our data scientists can interpret the data effectively and provide useful results and insights based on the analysis. There is a list of technical specifications which are needed. Ramp rates should be in the range of 1 degree Celsius to 100 degree Celsius per minute. The technique requires Nitrogen purged environment, and Nishka research scientific group takes care of all of the requirements. The temperature range should be between 30 degrees Celsius to 800 degrees Celsius. We follow all the specifications and the detection limit is calculated and analyzed. We make sure that the components are seen in the range of ppm.

Nishka Research

NISHKA has been helping customers unlock their full potential and realize their true value for more than 13 years by providing innovative and bespoke solutions to ensure the highest standards.
View More

Nishka Research Pvt. Ltd.

Regus Business Center,
4th floor, Gumidelli Commercial Complex,
1-10-39 to 44, Old Airport Road, Begumpet,
Hyderabad-500016
India

Phone : +91 40 29303155

Mobile : +91 7842798518

Send Mail : [email protected]
Copyright © 2023 -NISHKA Research Pvt. Ltd. |
Privacy Policy
apartmentdatabasedownloadchevron-down
Ajay Gunti
Ajay Gunti

Left us a 4 star review

Ajay Gunti
December 14, 2021
Andem Jhansi
December 14, 2021
Keyur Butani
May 10, 2022

Submitted the samples for my phd work . Great work and reports submited with 2 days of time . Also the image clarity and all data are clear .

Abhijit Patil
October 30, 2020

A very good lab delivering acurate results. I must also mention about the very cordial staff that they have.

Narendar Vemula
December 14, 2021
Raviteja. Vathsavai
December 17, 2021
akshay shriwas
December 14, 2021
Ramkumar Ganguly
April 25, 2022
Yedukondalu Janapuram
December 14, 2021
Anita Raj Panigrahi
October 20, 2021

Thank you for your services.. Looking forward for more collaboration with your labs for my future projects..

KESHAMONI AKHILAGOUD
December 14, 2021
Aishwarya Katrela
April 27, 2022
Firdose Begum
December 14, 2021
Divya Gaddam
December 15, 2021
Chaithanya Reddy
December 30, 2021
Samiksha More
June 2, 2022

Great work done by nishka research. Thank you so much for your kind Co operation

sai charan
April 30, 2022
VENKATESH PANTHIKI
December 14, 2021
sushma nampally
December 15, 2021
Sai teja Reddy
March 1, 2022
Tejaswini Kulakarni
December 14, 2021
M VENKAT M VENKAT
August 22, 2021
Sashi Kanth
October 12, 2020

I am a PhD scholar from Kaunas University at Lithuania, Europe. I have given a sample to perform SEM analysis of the organic tissue. The results are highly satisfactory and impressive. The service was really excellent, on time( even before the time schedule), consumer friendly. cost to the academic samples are very less comparing with others. Once again thanks to Nishka for providing me the service ontime as I am really in urgency...

Shyamala Mudiraj46
December 14, 2021
linkedin facebook pinterest youtube rss twitter instagram facebook-blank rss-blank linkedin-blank pinterest youtube twitter instagram